HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20446227, compound → HCID 20446171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20446227 | HCID 20446227 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20446171 | HCID 20446171 | — |
Reaction Steps
A mixture of 2-oxo-3-methylthio-7-(2-aminophenoxy)indoline (4.5 g.), Raney nickel (W-2 type)(9 ml.) and dioxane (50 ml.) was treated in a similar manner to that of the Preparation 15-(2) to give the captioned compound (3.5 g.) mp 210° to 212° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472433 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-c457461232a94a7c91ec0a80520b6c20 |
| Source note | uspto-grants-1984_09 |