HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20446168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20446231 | HCID 20446231 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20446168 | HCID 20446168 | 63.6% |
Reaction Steps
A mixture of ethyl 2-[2-amino-3-(3,4-dichlorphenoxy)phenyl]acetate (7.2 g.), sodium hydroxide (1.7 g.) and water (50 ml.) was treated in a similar manner to that of Example 5-(2). The resultant residue was pulverized with benzene, and the precipitates were collected by filtration and dried to give 2-[2-amino-3-(3,4-dichlorophenoxy)phenyl]acetic acid (4.2 g.). mp 125° to 127° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472433 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-837821fc120e42aa96db4c515f8612b4 |
| Source note | uspto-grants-1984_09 |