Ammonium Chloride → HCID 20446194, compound

HRID 2418395Notes

Reaction equation

HRID 2418395 reaction equation
[Cl-].[NH4+].[N+:3]([C:6]1[C:11]([O:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[Cl:19])=[CH:10][CH:9]=[CH:8][C:7]=1[CH2:20][C:21]([O:23]CC)=O)([O-])=O>C(O)C.O.[Fe]>[O:23]=[C:21]1[CH2:20][C:7]2[C:6](=[C:11]([O:12][C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=3[Cl:19])[CH:10]=[CH:9][CH:8]=2)[NH:3]1

Participants

6

Reactant 2

HCID 25517Ammonium ChlorideHCID 20446173HCID 20446173, compound

Product 1

HCID 20446194HCID 20446194, compound

Reagents, catalysts & solvents 3

HCID 23925IronCatalystHCID 702EthanolSolventHCID 962WaterSolvent

Procedure

A mixture of iron powder and ammonium chloride in ethanol and water and ethyl 2-[2-nitro-3-(2-chlorophenoxy)phenyl]acetate were treated in a similar manner to that of Preparation 28-(1) to give 2-oxo-7-(2-chlorophenoxy)indoline

Workup

  1. additionwere treated in a similar manner to that
  2. customof Preparation 28-(1)

Sources & evidence

ORD record
ord-8608154d93f147dba08eb69f98d55eea
Source dataset
uspto-grants-1984_09
Patent number
US04472433

Reaction notes

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