Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-(2,2,6,6-Tetramethylpiperidin-4-yl)azepan-2-one | HCID 18551435 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20446372 | HCID 20446372 | — |
Reaction Steps
Following the general procedure of Example 3, 12.1 g (0.05 mole) of the compound prepared in Example 1 is dissolved in 75 ml of N,N-dimethylformamide containing a suspension of 10.6 g (0.1 mole) of sodium carbonate. To this mixture is then added 14.6 g (0.05 mole) of allyl bromide and the reaction mixture is then heated at 80° C. for two hours. The solvent is then removed in vacuo and the residue is vacuum distilled at 171°-176° C./0.7 mm to give 7.6 g of the above named product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04472547 |
|---|
| Source dataset | uspto-grants-1984_09 |
|---|
| ORD ID | ord-b91a10d47f7542bb87dc3c47f058c968 |
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| Source note | uspto-grants-1984_09 |
|---|
