Benzaldehyde → HCID 10965718, compound

HRID 2418636Notes

Reaction equation

[CH:1](=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:9]([O:14][CH3:15])(=[O:13])[CH:10]([CH3:12])[CH3:11]>>[CH3:11][C:10]([CH3:12])([CH:1]([OH:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[C:9]([O:14][CH3:15])=[O:13]

Participants

Reactant 2

HCID 240Benzaldehyde

HCID 11039Methyl isobutyrate

Product 1

HCID 10965718HCID 10965718, compound

Procedure

A 50 milligram sample of the prepared hydroxy-ester is pyrolyzed in a sealed tube at 200° C. for 30 minutes. Analysis of the pyrolyzate by liquid chromatography indicates the following composition: 93% of unreacted starting material and 7% of a 1:1 mixture of benzaldehyde and methyl isobutyrate.

Sources & evidence

ORD record: ord-91e29c905f694b169c4f489c2ff3d596
Source dataset: uspto-grants-1984_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04473085

Reaction notes

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