HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Isothiocyanate → HCID 13339828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Isothiocyanate | HCID 2346 | — |
| Reactant | N-Phenylglycine | HCID 66025 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13339828 | HCID 13339828 | 20% |
Reaction Steps
A mixture containing 30.2 g (0.2 M) of N-phenyl glycine, 37.2 g (0.25M) of benzylisothiocyanate and 80 ml of toluene was refluxed for 5 hours and allowed to stand at room temperature overnight. The product was washed with toluene and recrystallized from ethanol to produce 12 g (0.04 mole) of the above-identified product having a melting point of 103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04473393 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-a5cf3dc600724936863c9aa43582757c |
| Source note | uspto-grants-1984_09 |