Cyclohexyl isothiocyanate → HCID 13339832, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of N-phenyl glycine (15.1 g, 0.1M) and cyclohexylisothiocyanate (21.2 g, 0.15M) was heated at 100° C. for 8 hours and then allowed to stand at room temperature overnight. The reaction mixture was placed in about 50 ml of ethanol, collected by filtration and recrystallized from ethanol to produce 11 grams (0.047M) of the above-identified product having a melting point of 156° C.

Provenance & Evidence