Methane → HCID 86739656, compound

Participants

Reaction Steps

A mixture of N-phenyl glycine (15.1 grams, 0.1 moles) and allylisothiocyanate (12.0 grams, 0.12 moles) was refluxed for 6 hours and allowed to stand overnight at room temperature (21° C.). The reaction mixture became a solid mass which was ground and crystallized from ethanol using charcoal, 7.26 grams (31% yield) of the above-identified product was recovered having a melting point of about 74° C.

Provenance & Evidence