Methyl Acrylate → HCID 20444819, compound

Participants

Reaction Conditions

Reaction Steps

While stirring at a temperature of 20° C., 90.3 grams (1.05 mole) of methylacrylate were dripped into 129 grams (1 mole) of 2-ethylhexylamine within a period of 30 minutes. The temperature was increased to 35° C. The mixture was stirred at 100° C. for 2 hours and was subsequently degassed at 50° C. under a high vacuum for 1 hour. The remaining residue was 210 grams (98 percent of theory) liquid N-(2'-carbomethoxy-ethyl)-2-ethylhexylamine. The 60 MHz-Nuclear Magnetic Resonance Spectrum s 3.7 ppm COOCH3 ; m 2.9 ppm; m 2.5 ppm; 0.7 to 1.5 ppm confirms the structure.

Provenance & Evidence