HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 178420830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 178476830 | HCID 178476830 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178420830 | HCID 178420830 | — |
Reaction Steps
To a solution of α-hydroxyethylphosphinic acid (330 mg) in methanol, a solution of morpholine (261 mg) in methanol (1 ml) was added, and the resultant mixture was stirred for 2 hours. After removal of methanol by distillation, there was obtained morpholinium α-hydroxyethylphosphinate (Compound No. 14) (556 mg). nD24.5 1.4621.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04473561 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-050e83265e134dbeb4402e03e19cc7ed |
| Source note | uspto-grants-1984_09 |