HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13339995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 88450-60-6 | HCID 13339988 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13339995 | HCID 13339995 | — |
Reaction Steps
A mixture of 13.9 g. of N-(2,4-dimethylbenzylidene)-2,4-dichloroaniline, 1.89 g. of sodium borohydride and 150 ml of ethanol is stirred under reflux for one hour, allowed to cool and poured into water. Recrystallization from ethanol yields N-(2,4-dimethylbenzyl)-2,4-dichloroaniline, m.p. 88°-90°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04473579 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-de7cd5887c054836bf4d3a27bf8b0c5c |
| Source note | uspto-grants-1984_09 |