Hydrochloric Acid → HCID 58103591, compound

Participants

Reaction Steps

(S)-N-((R)-cyclopropyl(6-(trifluoromethyl)pyridin-3-yl)methyl)-2-methylpropane-2-sulfinamide (0.245 g, 0.000765 mol), Ethanol (2.7 g, 0.059 mol), and 4.0 M of Hydrogen chloride in Dioxane (2.7 mL, 0.011 mol) are combined and stirred for 30 minutes. The mixture is allowed to stir overnight. The solvent is removed and the residue is dissolved in ethanol. After washing with ethanol 3 more times, the mixture is concentrated and the residue is dried under high vacuum overnight to obtain a solid.

Provenance & Evidence