HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 70624690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 70624630 | HCID 70624630 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 70624690 | HCID 70624690 | 85% |
Reaction Steps
0.14 mole of butyl bromide and 0.14 mole of N-hydroxy dodecenylsuccinimide are dissolved in 100 milliliters of dimethylformamide. 50 milliliters of triethylamine are added and the mixture is stirred overnight at room temperature. The solvent is then removed under vacuum and the reaction product is water washed until salt free and then dried. A yield of 85% of N-butoxy dodecenylsuccinimide is recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04104182 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-2edc3d5ad54641e49651bcc0596aeb30 |
| Source note | uspto-grants-1978_08 |