Butyl bromide → HCID 70624690, compound

HRID 2418952Notes

Reaction equation

HRID 2418952 reaction equation
[CH2:1](Br)[CH2:2][CH2:3][CH3:4].[OH:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH:17]=[CH:18][N:19]1[C:23](=[O:24])[CH2:22][CH2:21][C:20]1=[O:25].C(N(CC)CC)C>CN(C)C=O>[CH2:1]([O:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH:17]=[CH:18][N:19]1[C:23](=[O:24])[CH2:22][CH2:21][C:20]1=[O:25])[CH2:2][CH2:3][CH3:4]

Participants

5

Reactant 3

HCID 8002Butyl bromideHCID 8471TriethylamineHCID 70624630HCID 70624630, compound

Product 1

HCID 70624690HCID 70624690, compoundYield 85%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

0.14 mole of butyl bromide and 0.14 mole of N-hydroxy dodecenylsuccinimide are dissolved in 100 milliliters of dimethylformamide. 50 milliliters of triethylamine are added and the mixture is stirred overnight at room temperature. The solvent is then removed under vacuum and the reaction product is water washed until salt free and then dried. A yield of 85% of N-butoxy dodecenylsuccinimide is recovered.

Workup

  1. customThe solvent is then removed under vacuum
  2. washwashed until salt free
  3. customdried

Sources & evidence

ORD record
ord-2edc3d5ad54641e49651bcc0596aeb30
Source dataset
uspto-grants-1978_08
Patent number
US04104182

Reaction notes

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