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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2418982Generated: November 1, 2026

Hydrochloric Acid → HCID 20316441, compound

https://huagongshe.com/reaction/2418982

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 12443712HCID 12443712—
SolventIsoamyl AlcoholHCID 31260—
ProductHCID 20316441HCID 20316441—

Reaction Steps

A solution of 250 mg. of 10,11-dihydrodibenzo[b.f]thiepin-2-acetic acid in 30 ml. of isoamyl alcohol is saturated with hydrogen chloride. After 90 minutes, the excess alcohol is distilled off under reduced pressure to yield isoamyl 10,11-dihydrodibenzo[b.f]thiepin-2-acetate, which can be further purified by thin layer chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04104280
Source datasetuspto-grants-1978_08
ORD IDord-f07707b1f3824f7f8b85f00c0f5fed94
Source noteuspto-grants-1978_08