HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 23670399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 12443712 | HCID 12443712 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23670399 | HCID 23670399 | — |
Reaction Steps
A solution of 350 mg. of 10,11-dihydrodibenzo[b.f]-thiepin-2-acetic acid in five ml. of methanol is treated with 1.1 molar equivalents of 1N methanolic potassium hydroxide. The solvent is evaporated under reduced pressure and the residue taken up in 2 ml. of methanol, followed by precipitation with ether, to yield potassium 10,11-dihydrodibenzo[b.f]thiepin-2-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04104280 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-12047bbc02764a0a9ae7d50c0e4210cc |
| Source note | uspto-grants-1978_08 |