HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23333872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18965986 | HCID 18965986 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23333872 | HCID 23333872 | 91% |
Reaction Steps
Dry hydrogen chloride gas is introduced in a solution of 1.0 g (6 millimoles) of 1-aminotricyclo [4.3.1.12,5 ] undecane of formula (I) in 15 ml of anhydrous diethyl ether to form a white precipitate. The precipitate is filtered off, dried and recrystallized from acetone-methanol to obtain 1.1 g (yield: 91%) of 1-aminotricyclo [4.3.1.12,5 ] undecane hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04104305 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-82d2e425577b44a5acbbf959bc82fa29 |
| Source note | uspto-grants-1978_08 |