反应详情

Dry hydrogen chloride gas is introduced in a solution of 1.0 g (6 millimoles) of 1-aminotricyclo [4.3.1.12,5 ] undecane of formula (I) in 15 ml of anhydrous diethyl ether to form a white precipitate. The precipitate is filtered off, dried and recrystallized from acetone-methanol to obtain 1.1 g (yield: 91%) of 1-aminotricyclo [4.3.1.12,5 ] undecane hydrochloride.

1. customto form a white precipitate
2. filtrationThe precipitate is filtered off
3. customdried
4. customrecrystallized from acetone-methanol