Hydrochloric Acid → HCID 23333872, compound

HRID 2418987Notes

Reaction equation

HRID 2418987 reaction equation
[ClH:1].[NH2:2][C:3]12[CH2:12][CH:8]([CH2:9][CH2:10][CH2:11]1)[CH:7]1[CH2:13][CH:4]2[CH2:5][CH2:6]1>C(OCC)C>[ClH:1].[NH2:2][C:3]12[CH2:12][CH:8]([CH2:9][CH2:10][CH2:11]1)[CH:7]1[CH2:13][CH:4]2[CH2:5][CH2:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18965986HCID 18965986, compound

Product 1

HCID 23333872HCID 23333872, compoundYield 91%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Dry hydrogen chloride gas is introduced in a solution of 1.0 g (6 millimoles) of 1-aminotricyclo [4.3.1.12,5 ] undecane of formula (I) in 15 ml of anhydrous diethyl ether to form a white precipitate. The precipitate is filtered off, dried and recrystallized from acetone-methanol to obtain 1.1 g (yield: 91%) of 1-aminotricyclo [4.3.1.12,5 ] undecane hydrochloride.

Workup

  1. customto form a white precipitate
  2. filtrationThe precipitate is filtered off
  3. customdried
  4. customrecrystallized from acetone-methanol

Sources & evidence

ORD record
ord-82d2e425577b44a5acbbf959bc82fa29
Source dataset
uspto-grants-1978_08
Patent number
US04104305

Reaction notes

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