HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20313856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 20313842 | HCID 20313842 | — |
| Product | HCID 20313856 | HCID 20313856 | — |
Reaction Steps
A solution of N-(5-methoxy-1,3-benzodithiol-2-ylidene)benzenamine (4.5 g) in 100 ml of methyl iodide is heated at reflux for three days. The resultant precipitate is collected by filtration and recrystallized from acetonitrile/benzene to yield 6 g of the title compound, melting point 199° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04104467 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-b2830ff89052490aa29572b6cc920d80 |
| Source note | uspto-grants-1978_08 |