HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 20315174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 47132160 | HCID 47132160 | — |
| Product | HCID 20315174 | HCID 20315174 | 92.5% |
Reaction Steps
Treatment of 4-benzamido-1-(3-hydroxypropyl) piperidine with benzoyl chloride as in the previous example gave 3.4 grams (92.5% yield) of the title compound, m.p. 146°-7° C. Crystallisation from ethanolic hydrogen chloride afforded the hydrochloride, m.p. 211°-212° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04105666 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-557033e448bc4105b4aeffa9f49ee8da |
| Source note | uspto-grants-1978_08 |