HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54044700, compound → HCID 70617358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54044700 | HCID 54044700 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70617358 | HCID 70617358 | — |
Reaction Steps
A solution of 6.2 g of 4-(N-Methylacetamido)-3-[1-acetyl-2-(2,6-dichlorobenzylidene)hydrazino]-1,2,4-triazole in 50 ml of acetic acid, 50 ml of concentrated hydrochloric acid and 50 ml of water is heated at reflux overnight. The solution is evaporated and the residue is recrystallized from ethanolisopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04105768 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-f19250d53a6c4bc189cc4577c4a119e2 |
| Source note | uspto-grants-1978_08 |