HCID 54044700, compound → HCID 70617358, compound

HRID 2419309Notes

Reaction equation

HRID 2419309 reaction equation
[CH3:1][N:2]([N:6]1[CH:10]=[N:9][N:8]=[C:7]1[N:11](C(=O)C)[N:12]=[CH:13][C:14]1[C:19]([Cl:20])=[CH:18][CH:17]=[CH:16][C:15]=1[Cl:21])C(=O)C>C(O)(=O)C.Cl.O>[ClH:20].[Cl:21][C:15]1[CH:16]=[CH:17][CH:18]=[C:19]([Cl:20])[C:14]=1[CH:13]=[N:12][NH:11][C:7]1[N:6]([NH:2][CH3:1])[CH:10]=[N:9][N:8]=1

Participants

5

Reactant 1

HCID 54044700HCID 54044700, compound

Product 1

HCID 70617358HCID 70617358, compound

Reagents, catalysts & solvents 3

HCID 176Acetic AcidSolventHCID 313Hydrochloric AcidSolventHCID 962WaterSolvent

Procedure

A solution of 6.2 g of 4-(N-Methylacetamido)-3-[1-acetyl-2-(2,6-dichlorobenzylidene)hydrazino]-1,2,4-triazole in 50 ml of acetic acid, 50 ml of concentrated hydrochloric acid and 50 ml of water is heated at reflux overnight. The solution is evaporated and the residue is recrystallized from ethanolisopropyl ether.

Workup

  1. temperatureat reflux overnight
  2. customThe solution is evaporated
  3. customthe residue is recrystallized from ethanolisopropyl ether

Sources & evidence

ORD record
ord-f19250d53a6c4bc189cc4577c4a119e2
Source dataset
uspto-grants-1978_08
Patent number
US04105768

Reaction notes

Loading…