HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 20315597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Acetophenone, 4'-morpholinocarbonylmethoxy- | HCID 34762 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20315597 | HCID 20315597 | — |
Reaction Steps
A solution of bromine (8.0g.) in chloroform (30ml.) was added dropwise to a stirred solution of 4-(4-acetylphenoxyacetyl)morpholine (13.15g.) in chloroform (120ml.) at 35° C. After 1 hour, the reaction mixture was filtered and the filtrate was washed with water (2 × 30ml.), dried and evaporated. The residue was recrystallised from methanol/ether to give 4-[4-(bromoacetyl)phenoxyacetyl]morpholine, m.p. 105°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04105790 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-85740456960642d68192ad4be19c2414 |
| Source note | uspto-grants-1978_08 |