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HRID2419439

反应详情

EQUATION

反应方程式

HRID 2419439 的结构方程式

REACTANTS

反应物

2
结构：OC(c1ccccc1)c1ccccc1
HCID7037

Benzhydrol

C13H12O

结构：O=C(O)[C@@H]1CCCN1C(=O)C(CS)Cc1ccccc1
HCID18397285

1-[3-Phenyl-2-(sulfanylmethyl)propanoyl]-L-proline

C15H19NO3S

PRODUCTS

生成物

1
结构：O=C(O)[C@@H]1CCCN1C(=O)C(CSC(c1ccccc1)c1ccccc1)Cc1ccccc1
HCID54380838

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=C(O)C(F)(F)F
溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

Diphenylmethanol (0.92 g) and 1-(3-mercapto-2-benzylpropanoyl)-L-proline (1.5 g) are dissolved in trifluoroacetic acid (10 ml) and the solution is kept at room temperature for 30 minutes. The excess trifluoroacetic acid is removed in vacuo to yield 1-[3-[(diphenylmethyl)thio]-2-benzylpropanoyl]-L-proline.

WORKUP

后处理

  1. customThe excess trifluoroacetic acid is removed in vacuo