HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloronicotinoyl Chloride → HCID 58563708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Reactant | 4-oxo-4H,5H,6H,7H-pyrazolo[1,5-a]pyridine-2- carboxylic acid | HCID 22605322 | — |
| Product | HCID 58563708 | HCID 58563708 | — |
Reaction Steps
A-07 is prepared using general procedure A2 starting from 4-oxo-4,5,6,7-tetrahydro-pyrazolo[1,5-a]pyridine-2-carboxylic acid (5.00 g, 27.8 mmol) and 6-chloro-nicotinoyl chloride (7.33 g, 41.6 mmol). Yield: 7.37 g. HPLC-MS: Rt=1.94 min, (M+H)+=320/322.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653097B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-ff73af7f0a40498bb500273296d61807 |
| Source note | uspto-grants-2014_02 |