HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 54222234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Hydrofluoric Acid | HCID 14917 | — |
| Reactant | HCID 13434000 | HCID 13434000 | — |
| Product | HCID 54222234 | HCID 54222234 | 52% |
Reaction Steps
105 g (0.5 mol) of 2-chloromethylphenyl chloroformate are warmed to 40° C with 195 g (2.5 mols) of benzene in 100 ml of hydrogen fluoride for one hour and to 100° C for a further hour. After distillation in vacuo, 60 g (yield: 52%) of 2-benzylphenyl fluoroformate are obtained. 2nd reaction stage
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107186 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-8e6da21ca1ff4775870ed7d8270f8bb9 |
| Source note | uspto-grants-1978_08 |