Furfurylamine → HCID 12493316, compound

HRID 2419644Notes

Reaction equation

HRID 2419644 reaction equation
CS[C:3]1[N:8]2[CH:9]=[CH:10][N:11]=[C:7]2[CH:6]=[N:5][N:4]=1.[CH2:12]([NH2:18])[C:13]1[O:17][CH:16]=[CH:15][CH:14]=1>>[CH2:12]([NH:18][C:3]1[N:8]2[CH:9]=[CH:10][N:11]=[C:7]2[CH:6]=[N:5][N:4]=1)[C:13]1[O:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 3438FurfurylamineHCID 124933105-(Methylthio)-imidazo[1,2-d]-as-triazine

Product 1

HCID 12493316HCID 12493316, compound

Procedure

A 5.0 gm. portion of 5-(methylthio)-imidazo[1,2-d]-as-triazine is combined with 45 ml. of furfurylamine and refluxed for 2 hours. The mixture is allowed to stand at room temperature overnight. The gummy solid is collected and crystallized from 60 ml. of hot methanol, giving 2.75 gm. of the desired product as crystals, m.p. 212°-214° C.

Workup

  1. customThe gummy solid is collected
  2. customcrystallized from 60 ml
  3. customof hot methanol, giving 2.75 gm

Sources & evidence

ORD record
ord-664eda491cf44ff4b2bbf904d8eab2c2
Source dataset
uspto-grants-1978_08
Patent number
US04107309

Reaction notes

Loading…