Diphenyl Ether → HCID 13548750, compound

HRID 2419656Notes

Reaction equation

C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[CH:9][NH:10][C:11]=1[CH3:12].C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:12][C:11]1[N:10]=[CH:9][N:8]2[C:7]=1[CH:6]=[N:5][NH:4][C:3]2=[S:2]

Participants

Reactant 2

HCID 7583Diphenyl Ether

HCID 135987371HCID 135987371, compound

Product 1

HCID 13548750HCID 13548750, compound

Procedure

A suspension of 14.39 gm. of 3-(5-methyl-4-imidazolylmethylene)dithiocarbazic acid methyl ester in 100 ml. of diphenyl ether is reacted as described in Example 23 giving the desired product as yellow crystals, m.p. 262°-268° C.

Workup

additionA suspension of 14.39 gm

Sources & evidence

ORD record: ord-9d7fdccce8b1495c8536e9f9b0e32338
Source dataset: uspto-grants-1978_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04107308

Reaction notes

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