Diphenyl Ether → HCID 12493299, compound

HRID 2419657Notes

Reaction equation

HRID 2419657 reaction equation
C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([CH2:12][CH2:13][CH3:14])[NH:10][CH:11]=1.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH2:12]([C:9]1[N:8]2[C:3](=[S:2])[NH:4][N:5]=[CH:6][C:7]2=[CH:11][N:10]=1)[CH2:13][CH3:14]

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 178440134HCID 178440134, compound

Product 1

HCID 12493299HCID 12493299, compound

Procedure

A 102.2 gm. portion of 3-(2-n-propyl-4-imidazolylmethylene)dithiocarbazic acid methyl ester in 500 ml. of diphenyl ether is reacted as described in Example 23 giving the desired product as a white solid, m.p. 201.5°-203.5° C.

Sources & evidence

ORD record
ord-c9495b7b41f1438e96dae6ff5b7d42f9
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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