Methyl iodide → HCID 13548775, compound

HRID 2419663Notes

Reaction equation

HRID 2419663 reaction equation
[CH2:1]([C:4]1[N:8]2[C:9](=[S:13])[NH:10][N:11]=[CH:12][C:7]2=[CH:6][N:5]=1)[CH2:2][CH3:3].[Na].[CH3:15]I>CO>[CH2:1]([C:4]1[N:8]2[C:9]([S:13][CH3:15])=[N:10][N:11]=[CH:12][C:7]2=[CH:6][N:5]=1)[CH2:2][CH3:3]

Participants

5

Reactant 3

HCID 6328Methyl iodideHCID 5360545SodiumHCID 12493299HCID 12493299, compound

Product 1

HCID 13548775HCID 13548775, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A 3.98 gm. portion of 6-n-propyl-imidazo[1,5-d]-as-triazine-4(3H)-thione is added to a solution of 0.46 gm. of sodium in 15 ml. of methanol under nitrogen. A 1.56 ml. portion of methyl iodide is added. The reaction procedes as described in Example 30 giving the desired product, m.p. 132°-134° C.

Sources & evidence

ORD record
ord-74aed4ecdd71454fb8d05f643fb66bdf
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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