HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 13548776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 13548750 | HCID 13548750 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13548776 | HCID 13548776 | — |
Reaction Steps
A 1.66 gm. portion of 8-methyl-imidazo[1,5-d]-as-triazine-4(3H)-thione is added to a solution of 0.23 gm. of sodium in 10 ml. of methanol. A 0.75 ml. portion of methyl iodide is added, the mixture is allowed to stand for 30 minutes and then evaporated to dryness. The product is chromatographed on a silica gel column. The appropriate fractions are recrystallized from acetone giving the desired product, m.p. 128°-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107308 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-3984c2e3277b4e4da592c684d9e46491 |
| Source note | uspto-grants-1978_08 |