Methyl iodide → HCID 20314263, compound

HRID 2419665Notes

Reaction equation

[CH3:1][C:2]1[N:6]2[C:7](=[S:11])[NH:8][N:9]=[CH:10][C:5]2=[C:4]([CH3:12])[N:3]=1.[CH2:13](I)[CH3:14].C1C2N(C=NC=2)C(=S)NN=1.CI>>[CH3:1][C:2]1[N:6]2[C:7]([S:11][CH2:13][CH3:14])=[N:8][N:9]=[CH:10][C:5]2=[C:4]([CH3:12])[N:3]=1

Participants

Reactant 4

HCID 6328Methyl iodide

HCID 6340Iodoethane

HCID 12493298HCID 12493298, compound

HCID 13548755HCID 13548755, compound

Product 1

HCID 20314263HCID 20314263, compound

Procedure

The procedure of Example 29 is repeated substituting equimolecular amounts of 6,8-dimethyl-imidazo[1,5-d]-as-triazine-4(3H)-thione and ethyl iodide for the imidazo[1,5-d]-as-triazine-4(3H)-thione and methyl iodide employed in that example. There is thus obtained the title compound in equally good yield.

Sources & evidence

ORD record: ord-da19b4e2cba54f6f9695448423c04123
Source dataset: uspto-grants-1978_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04107308

Reaction notes

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