HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 20314273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 12493298 | HCID 12493298 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20314273 | HCID 20314273 | — |
Reaction Steps
A 15.2 gm. portion of imidazo[1,5-d]-as-triazine-4(3H)-thione in 75 ml. of methanol is treated with 2.3 gm. of sodium in 75 ml. of methanol. After 5 minutes, a 12.0 gm. portion of allyl bromide is added and the reaction is continued as described in Example 29 giving the desired product, m.p. 68°-69.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107308 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-5cd48f01b91f4ea8bdeba317b530d295 |
| Source note | uspto-grants-1978_08 |