Allyl bromide → HCID 20314273, compound

HRID 2419667Notes

Reaction equation

HRID 2419667 reaction equation
[CH:1]1[C:2]2[N:3]([CH:8]=[N:9][CH:10]=2)[C:4](=[S:7])[NH:5][N:6]=1.[Na].[CH2:12](Br)[CH:13]=[CH2:14]>CO>[CH2:14]([S:7][C:4]1[N:3]2[CH:8]=[N:9][CH:10]=[C:2]2[CH:1]=[N:6][N:5]=1)[CH:13]=[CH2:12]

Participants

5

Reactant 3

HCID 7841Allyl bromideHCID 5360545SodiumHCID 12493298HCID 12493298, compound

Product 1

HCID 20314273HCID 20314273, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

A 15.2 gm. portion of imidazo[1,5-d]-as-triazine-4(3H)-thione in 75 ml. of methanol is treated with 2.3 gm. of sodium in 75 ml. of methanol. After 5 minutes, a 12.0 gm. portion of allyl bromide is added and the reaction is continued as described in Example 29 giving the desired product, m.p. 68°-69.5° C.

Sources & evidence

ORD record
ord-5cd48f01b91f4ea8bdeba317b530d295
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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