1-Methylpiperazine → HCID 13548818, compound

HRID 2419671Notes

Reaction equation

HRID 2419671 reaction equation
CS[C:3]1[N:8]2[CH:9]=[N:10][CH:11]=[C:7]2[CH:6]=[N:5][N:4]=1.[CH3:12][N:13]1[CH2:18][CH2:17][NH:16][CH2:15][CH2:14]1>C1(C)C=CC=CC=1>[CH3:12][N:13]1[CH2:18][CH2:17][N:16]([C:3]2[N:8]3[CH:9]=[N:10][CH:11]=[C:7]3[CH:6]=[N:5][N:4]=2)[CH2:15][CH2:14]1

Participants

4

Reactant 2

HCID 531671-MethylpiperazineHCID 12493309HCID 12493309, compound

Product 1

HCID 13548818HCID 13548818, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A mixture of 0.83 gm. of 4-(methylthio)-imidazo[1,5-d]-as-triazine, 5.0 gm. of N-methylpiperazine and 8 ml. of toluene is reacted as described in Example 40 giving the desired product, m.p. 163°-166° C.

Workup

  1. additionA mixture of 0.83 gm

Sources & evidence

ORD record
ord-c7977afbc3ae45d684948e1b78f8b026
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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