HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzhydrylpiperazine → HCID 13548819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzhydrylpiperazine | HCID 70048 | — |
| Reactant | HCID 12493309 | HCID 12493309 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 13548819 | HCID 13548819 | — |
Reaction Steps
A solution of 6.68 gm of 4-(methylthio)-imidazo[1,5-d]-as-triazine, 15.1 gm of N-diphenylmethylpiperazine and 50 ml of xylene is refluxed for 19 hours. Upon evaporation to dryness, the residue is chromatographed on a silica gel dry column. The product is recrystallized from ethanol and has a melting point equal to 192°-193° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107308 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-eaa1701156fb48f193a29cacb7dcab2a |
| Source note | uspto-grants-1978_08 |