Benzylamine → HCID 13548820, compound

HRID 2419684Notes

Reaction equation

HRID 2419684 reaction equation
CS[C:3]1[N:8]2[CH:9]=[N:10][CH:11]=[C:7]2[CH:6]=[N:5][N:4]=1.[CH2:12]([NH2:19])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C1(C)C=CC=CC=1>[CH2:12]([NH:19][C:3]1[N:8]2[CH:9]=[N:10][CH:11]=[C:7]2[CH:6]=[N:5][N:4]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 7504BenzylamineHCID 12493309HCID 12493309, compound

Product 1

HCID 13548820HCID 13548820, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A solution of 16.6 g of 4-(methylthio)imidazo[1,5-d]-as-triazine, 51.3 ml (50.3 g) of benzylamine and 580 ml of toluene is refluxed for 10 days. After cooling, a precipitate is collected and recrystallized from methanol to yield the desired product, m.p. 275°-278° C.

Workup

  1. temperatureAfter cooling
  2. customa precipitate is collected
  3. customrecrystallized from methanol

Sources & evidence

ORD record
ord-04f2c0dd77934c68853a9f4ddd094e4e
Source dataset
uspto-grants-1978_08
Patent number
US04107308

Reaction notes

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