HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 13548820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 12493309 | HCID 12493309 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13548820 | HCID 13548820 | — |
Reaction Steps
A solution of 16.6 g of 4-(methylthio)imidazo[1,5-d]-as-triazine, 51.3 ml (50.3 g) of benzylamine and 580 ml of toluene is refluxed for 10 days. After cooling, a precipitate is collected and recrystallized from methanol to yield the desired product, m.p. 275°-278° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107308 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-04f2c0dd77934c68853a9f4ddd094e4e |
| Source note | uspto-grants-1978_08 |