HRID2419694

反应详情

EQUATION

反应方程式

HRID 2419694 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A 130 gm. portion of salicylamide in 500 ml. of ethanol is reacted with 52.4 gm. of sodium methoxide and 164.9 gm. of 1-iodopropane by heating at reflux. The mixture is cooled, precipitated in 1500 ml. of water and the solid is recrystallized from hot ethanol giving o-propoxybenzamide.

WORKUP

后处理

  1. temperatureat reflux
  2. temperatureThe mixture is cooled
  3. customprecipitated in 1500 ml
  4. customof water and the solid is recrystallized from hot ethanol