Diphenyl Ether → HCID 13548751, compound

HRID 2419726Notes

Reaction equation

HRID 2419726 reaction equation
C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[NH:10][CH:11]=1.C1(OC2C=CC=CC=2)C=CC=CC=1>>[C:12]1([C:9]2[N:8]3[C:3](=[S:2])[NH:4][N:5]=[CH:6][C:7]3=[CH:11][N:10]=2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 178504097HCID 178504097, compound

Product 1

HCID 13548751HCID 13548751, compound

Procedure

A suspension of 7.05 gm. of 3-(2-phenyl-4-imidazolylmethylene)dithiocarbazic acid methyl ester in 100 ml. of diphenyl ether is reacted as described in Example 58 giving the desired product, m.p. 210° C.

Workup

  1. additionA suspension of 7.05 gm

Sources & evidence

ORD record
ord-51a88a792c2f472893b873ebc81df657
Source dataset
uspto-grants-1978_08
Patent number
US04107307

Reaction notes

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