Diphenyl Ether → HCID 12493303, compound
Reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([CH2:13][CH2:14][CH3:15])[NH:11][CH:12]=1)C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH2:13]([C:10]1[N:9]2[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]2=[CH:12][N:11]=1)[CH2:14][CH3:15]Participants
3
Procedure
An 8.75 gm. portion of 3-(2-n-propyl-4-imidazolylmethylene)carbazic acid ethyl ester in 50 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product, m.p. 159°-162.5° C.
Sources & evidence
- ORD record
- ord-a66957a661e64f91b70f631ad5d3779e
- Source dataset
- uspto-grants-1978_08
- Patent number
- US04107307
Reaction notes
Loading…