Diphenyl Ether → HCID 12493304, compound

HRID 2419740Notes

Reaction equation

HRID 2419740 reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([C:13]([CH3:16])([CH3:15])[CH3:14])[NH:11][CH:12]=1)C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[C:13]([C:10]1[N:9]2[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]2=[CH:12][N:11]=1)([CH3:16])([CH3:15])[CH3:14]

Participants

3

Procedure

A 6.15 gm. portion of 3-(2-tert-butyl-4-imidazolylmethylene)carbazic acid ethyl ester in 40 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product, m.p. 186°-188° C.

Sources & evidence

ORD record
ord-bdf90c1cc59f44f7990c410ff4d8a7b7
Source dataset
uspto-grants-1978_08
Patent number
US04107307

Reaction notes

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