Diphenyl Ether → HCID 12493307, compound
Reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([C:14]([CH3:17])([CH3:16])[CH3:15])[NH:11][C:12]=1[CH3:13])C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[C:14]([C:10]1[N:9]2[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]2=[C:12]([CH3:13])[N:11]=1)([CH3:17])([CH3:16])[CH3:15]Participants
3
Procedure
A mixture of 5.11 gm. of 3-[(2-tert-butyl-5-methyl-4-imidazolyl)methylene]carbazic acid ethyl ester and 50 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product, m.p. 198°-200° C.
Workup
- additionA mixture of 5.11 gm
Sources & evidence
- ORD record
- ord-a9ecc47404a445f9abcf37b1ae4e097f
- Source dataset
- uspto-grants-1978_08
- Patent number
- US04107307
Reaction notes
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