HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 86735929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 4-Ethyl-3-thiosemicarbazide | HCID 1551780 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86735929 | HCID 86735929 | — |
Reaction Steps
A stirred solution of 97.0 g. of 4-ethyl-3-thiosemicarbazide and 127.8 g. of ethyl iodide in 500 ml. of ethanol is heated under reflux for 18 hours. The reaction mixture is concentrated under reduced pressure, diluted with n-hexane and filtered, giving the desired product as a nearly colorless solid, m.p. 73°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107326 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-e0776027656244c8bee7a5346ac006f6 |
| Source note | uspto-grants-1978_08 |