HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminothiazole → HCID 178522565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminothiazole | HCID 2155 | — |
| Reactant | HCID 178470066 | HCID 178470066 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 178522565 | HCID 178522565 | 78.1% |
Reaction Steps
A mixture of 6.02 g of the product of Step C, 200 ml of xylene, 2 g of 2-amino-thiazole and 20 g of siliporite NK20 was refluxed for 2 hours and the resulting product was crystallized from acetic acid to obtain 5.54 g of N-(2-thiazolyl)-2,4-dihydroxy-8-trifluoromethyl-quinoline-3-carboxamide in the form of colorless crystals melting at 260° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107310 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-cc831e694d44413c85ca88f7a3ed6764 |
| Source note | uspto-grants-1978_08 |