Phosphorus pentachloride → 64321-99-9

HRID 2419828Notes

Reaction equation

HRID 2419828 reaction equation
[F:1][C:2]([F:19])([F:18])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10](=O)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.P(Cl)(Cl)(Cl)(Cl)[Cl:21]>C1(C)C=CC=CC=1>[F:1][C:2]([F:19])([F:18])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]=[C:10]([Cl:21])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 2

HCID 24819Phosphorus pentachlorideHCID 137262N-[2-(Trifluoromethyl)phenyl]benzamide

Product 1

HCID 1419645764321-99-9Yield 101.5%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Using the procedure of Step B of Example 6, 26.52 g of the product of Step A and 22.9 g of phosphorus pentachloride were reacted in 160 ml of dry toluene to obtain 28.8 g of N-(2-trifluoromethylphenyl)-benzenecarboximidoyl chloride as an oil which was used as is for the next step.

Sources & evidence

ORD record
ord-f614707cbf3a40ff80732d69ed887b8f
Source dataset
uspto-grants-1978_08
Patent number
US04107310

Reaction notes

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