HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → 64321-99-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2'-Trifluoromethylbenzanilide | HCID 137262 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 64321-99-9 | HCID 14196457 | 101.5% |
Reaction Steps
Using the procedure of Step B of Example 6, 26.52 g of the product of Step A and 22.9 g of phosphorus pentachloride were reacted in 160 ml of dry toluene to obtain 28.8 g of N-(2-trifluoromethylphenyl)-benzenecarboximidoyl chloride as an oil which was used as is for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107310 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-f614707cbf3a40ff80732d69ed887b8f |
| Source note | uspto-grants-1978_08 |