HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178468496, compound → HCID 178524032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178468496 | HCID 178468496 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178524032 | HCID 178524032 | 77.7% |
Reaction Steps
Using the procedure of Step E of Example 6, 12.64 g of the product of Step D in 35 ml of 36° Be sodium hydroxide and 70 ml of 95% ethanol were refluxed for 51/2 hours to obtain 9.06 g of 4-hydroxy-2-phenyl-8-trifluoromethyl-quinoline-3-carboxylic acid melting at 204° C which was used as is for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107310 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-6f0f98a2252b46b88c9f00e1f6dd750c |
| Source note | uspto-grants-1978_08 |