HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 13384245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 13384246 | HCID 13384246 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13384245 | HCID 13384245 | — |
Reaction Steps
A solution of (±)-2-[4-(4-chlorophenyl)phenoxy]-3,3,3-trifluoro-2-methylpropionic acid (3.0 g.) in ether (100 ml.) is treated with an excess of ethereal diazomethane at 0° C. The solvent is evaporated and the residue recrystallised from methanol to give (±)-methyl 2-[4-(4-chlorophenyl)phenoxy]-3,3,3-trifluoro-2-methylpropionate, m.p. 87°-88° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04107329 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-adef97e96fb449c9970ff11b7e2efb18 |
| Source note | uspto-grants-1978_08 |