HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1-Methylethylidene)cyclohexanone → HCID 12220944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1-Methylethylidene)cyclohexanone | HCID 26252 | — |
| Reactant | HCID 20312280 | HCID 20312280 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12220944 | HCID 12220944 | — |
Reaction Steps
3,4-Dihydroisoquinolinium perchlorate (4.6 g) and 2-isopropylidenecyclohexanone (3 g) were dissolved in dimethylforamide (12 ml) and refluxed for 12 hours. The reaction mixture was cooled, diluted with ethanol, and filtered. The product was purified by recrystallization from methanol. Yield 3 g; m.p. 205°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04108667 |
| Source dataset | uspto-grants-1978_08 |
| ORD ID | ord-27135de797264b0ea899086a2a137f3e |
| Source note | uspto-grants-1978_08 |